Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography

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Published: Dec 30, 2006
DOI: https://doi.org/10.26850/1678-4618eqj.v31.4.2006.p55-58
Keywords:
Rubiaceae, Alibertia sessilis, enantiomeric aglycone lignans, HPLC

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Viviane Cândida da Silva
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Geraldo Humberto Silva
Universidade Federal de Sergipe, Departamento de Química, Aracajú, Brasil.
Vanderlan da Silva Bolzani
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Márcia Nasser Lopes
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.

Abstract

Enantiomeric aglycone lignans contained in a mixture were separated from a fraction of the extract of the stems of Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography. An efficient and fast separation can be achieved with methanol-water (30:70, v/v). Their structures were identified as (+)-lyoniresinol 3alpha-O-beta-glucopyranoside and (-)-lyoniresinol 3alpha-O-beta-glucopyranoside, being reported for the first time in Rubiaceae.

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How to Cite
da Silva, V. C., Silva, G. H., Bolzani, V. da S., & Lopes, M. N. (2006). Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography. Eclética Química, 31(4), 55–58. https://doi.org/10.26850/1678-4618eqj.v31.4.2006.p55-58
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Vol. 31 No. 4 (2006): Eclética Química
Section
Original articles
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