Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions

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Published: Sep 26, 2005
DOI: https://doi.org/10.26850/1678-4618eqj.v30.3.2005.p07-13
Keywords:
bivalent transition metals, 3-methoxybenzoate, thermal behaviour

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Adriana Cossu Vallejo
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Adriano Buzutti de Siqueira
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Érica Alvarenga Crespo Rodrigues
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Elias Yuki Ionashiro
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Gilbert Bannach
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.
Massao Ionashiro
Universidade Estadual Paulista, Instituto de Química, Araraquara, Brasil.

Abstract

Solid-state M-3-MeO-Bz compounds, where M stands for bivalent Mn, Co, Ni, Cu and Zn and
3-MeO-Bz is 3-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential
thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared
spectroscopy, and chemical analysis were used to characterize and to study the thermal behaviour of these
compounds. The results led to information about the composition, dehydration, thermal stability and
thermal decomposition of the isolated compounds.

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How to Cite
Vallejo, A. C., de Siqueira, A. B., Rodrigues, Érica A. C., Ionashiro, E. Y., Bannach, G., & Ionashiro, M. (2005). Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions. Eclética Química, 30(3), 07–13. https://doi.org/10.26850/1678-4618eqj.v30.3.2005.p07-13
Issue
Vol. 30 No. 3 (2005): Eclética Química
Section
Original articles
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